Unlocking the Secrets Behind the Resin-Gel Synthesis for the Controlled  Formation of Anatase and Rutile

Franklyn, P.J.; Narrandes, A.

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Title	Unlocking the Secrets Behind the Resin-Gel Synthesis for the Controlled Formation of Anatase and Rutile
Authors	Franklyn, P.J. Narrandes, A.
ORCID
Keywords	Titania Resin-Gel PEG XRD TEM Flame Synthesis
Type	Conference Papers
Date of Issue	2012
URI	http://essuir.sumdu.edu.ua/handle/123456789/34944
Publisher	Sumy State University
License	Copyright not evaluated
Citation	Franklyn, P.J. Unlocking the Secrets Behind the Resin-Gel Synthesis for the Controlled Formation of Anatase and Rutile [Текст] / P.J. Franklyn, A. Narrandes // Nanomaterials: Applications & Properties (NAP-2012) : 2-nd International conference, Alushta, the Crimea, September 17-22, 2012 / Edited by: A. Pogrebnjak. - Sumy : Sumy State University, 2012. - V.1, No1. - 01PCN40
Abstract	Resin-gel synthesis has the ability to become a powerful technique for the synthesis of multi-phase nanoparticles. This study aimed to take further steps into investigating the mechanism of the resin-gel synthesis based on phase differentiation of titania, in the hope to describe optimal synthetic conditions for desired polymorph production with tailored particle size. Solvent, polymer chain length, heating rate and the use of citric acid has been varied previously. The results obtained suggested that the working theory of the resin-gel synthesis may be incorrect as there was significant phase differentiation based on the solvent used. This work explored the effects of the stoichiometric ratio of PEG to TiCl4 and the effect of heating rates to clarify the reaction mechanism. When you are citing the document, use the following link http://essuir.sumdu.edu.ua/handle/123456789/34944
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