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Title | The Effect of Nano-SiO2 on the Structural, Electrical and Magnetic Properties of SiO2-LiFe5O8 Glass–ceramics Prepared by Sol Gel Auto-combustion Processing |
Authors |
Shash, N.M.
Rashad, M.M. El-Shaarawy, M.G. Maklad, M.H. Afifi, F.A. |
ORCID | |
Keywords |
Spinel ferrite Combustion synthesis Microstructure Electrical properties Magnetic properties |
Type | Conference Papers |
Date of Issue | 2015 |
URI | http://essuir.sumdu.edu.ua/handle/123456789/42712 |
Publisher | Sumy State University |
License | |
Citation | The Effect of Nano-SiO2 on the Structural, Electrical and Magnetic Properties of SiO2-LiFe5O8 Glass–ceramics Prepared by Sol Gel Auto-combustion Processing [Текст] / M.M. Rashad, N.M. Shash, M.G. El-Shaarawy et al. // Nanomaterials: Applications & Properties (NAP-2015) : Proceedings of the International Conference. — Sumy : Sumy State University, 2015. — V.4, No1. — 01MFPM05. |
Abstract |
The glass–ceramic with the composition x(LiFe5O8)/(100 – x) SiO2 (x = 20, 30, 40, 50, 100 wt. % ) were prepared by sol gel auto-combustion method. The influence of the SiO2 ratio in the glass-ceramics strucure prepared was investigated by X-ray diffraction (XRD) and scanning electron microscopy (SEM). Crystalline phases (LiFe5O8, SiO2, Fe2O3) were observed by X-ray powder diffraction in the glasses annealed at 800°C
for 2h. The crystallite size was found to increase from 27.29 nm (x = 20%) to 91.48 nm(x = 100 %). The microstructure of the formed powders was SiO2 ratio dependent. Increasing the SiO2 ratio was found to inhibit the grain growth of the formed ferrite. The electrical conductivity of glass-ceramics samples were raised with increasing the concentration of SiO2 ratio as the result of increasing the hopping of electrons between
Fe2+ and Fe3+ ions. The magnetic characteristics of the prepared glass ceramics were performed using a vibrating sample magnetometer in function of the magnetic field. The samples heat -treated at 800°C for 2h present a ferrimagnetic behavior. Alongside, the formed crystalline silicate lithium ferrite had good magnetic properties. High saturation magnetization (51.9 emu/g) was attained the formed ferrite sample of x = 100 % ratio annealed at 800°C for 2h. |
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File | Size | Format | Downloads |
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Shash.pdf | 1.01 MB | Adobe PDF | 338453637 |
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