A Simple Sonochemical Synthesis of Nanosized ZnO from Zinc Acetate and Sodium Hydroxide

Zakirov, M.I.; Semen’ko, M.P.; Korotchenkov, O.A.

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Title	A Simple Sonochemical Synthesis of Nanosized ZnO from Zinc Acetate and Sodium Hydroxide
Authors	Zakirov, M.I. Semen’ko, M.P. Korotchenkov, O.A.
ORCID
Keywords	semiconductors chemical synthesis phosphors x-ray diffraction
Type	Article
Date of Issue	2018
URI	http://essuir.sumdu.edu.ua/handle/123456789/71501
Publisher	Sumy State University
License	Copyright not evaluated
Citation	Zakirov, M.I. A Simple Sonochemical Synthesis of Nanosized ZnO from Zinc Acetate and Sodium Hydroxide / M.I. Zakirov, M.P. Semen'ko, O.A. Korotchenkov // Журнал нано- та електронної фізики. - 2018. - Т.10, № 5. - 05023. - DOI: 10.21272/jnep.10(5).05023
Abstract	An efficient sonochemical route for synthesis of nano sized zinc oxide is reported. The method employs zinc acetate and sodium hydroxide as precursors with isopropyl alcohol as a solvent. As prepared powders were characterized by XRD, SEM and FTIR. These show that the resulting powder is composed of multidomain crystallites of ZnO wurtzite, zincite and Zn(OH)2. The XRD-measured coherent domain size varies from about 20 to 30 nm, whereas SEM exhibits  200 nm crystallites. The wurtzite phase is found to dominate at sonication times smaller than  30 min. It is also found that the powders produced sonochemically exhibit smaller and narrower size-distributed particles compared to that in hydrothermally prepared powders.
Appears in Collections:	Журнал нано- та електронної фізики (Journal of nano- and electronic physics)