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Title Study of Structural and Optical Properties of FeS2 Nanoparticles Prepared by Polyol Method
Authors Chandrawat, G.S.
Tripathi, J.
Sharma, A.
Singh, J.
Tripathi, S.
Chouhan, Jyotsna
ORCID
Keywords nanoparticles
Polyol method
XRD
FTIR
Raman
Type Article
Date of Issue 2020
URI https://essuir.sumdu.edu.ua/handle/123456789/77368
Publisher Sumy State University
License
Citation Study of Structural and Optical Properties of FeS2 Nanoparticles Prepared by Polyol Method [Текст] / G.S. Chandrawat, J. Tripathi, A. Sharma [et al.] // Журнал нано- та електронної фізики. – 2020. – Т. 12, № 2. – 02016. – DOI: 10.21272/jnep.12(2).02016.
Abstract FeS2 nanoparticles were prepared using a simple and cost-effective Polyol method with ethylene glycol and precursor thiourea as capping reagents. The crystalline structure of FeS2 nanoparticles were confirmed by X-ray diffraction. Dimensions of the unit cell and Pa-3 space group were determined by Rietveld refinement. The average crystallite size was found to be ~ 42.1 nm. The stoichiometry of these nanoparticles were also confirmed by, Raman and Fourier Transform Infrared Spectroscopy. Further, Raman spectroscopy revealed the chemical bonding and symmetry of molecules. FTIR spectroscopy exhibited the presence of functional groups of Fe=S, Fe–S and S–S in the samples. Advanced measurements and analysis towards the applicability of surfactant coated pyrite FeS2 nanoparticles for solar cell etc. applications are in progress.
Appears in Collections: Журнал нано- та електронної фізики (Journal of nano- and electronic physics)

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