|Title||High pressure torsion of nickel powders obtained by electrodeposition|
|Date of Issue||2011|
|Publisher||Sumy State University|
|Citation||High pressure torsion of nickel powders obtained by electrodeposition [Текст] / L. D. Rafailovic, C. Rentenberger, A. Gavrilovic et al. // Nanomaterials: applications & properties. Proceedings : 1-st International conference, Alushta, Crimea, 27-30 Semptember 2011 / Edited by: A. Pogrebnjak, T. Lyutyy, S. Protsenko. — Sumy : Sumy State University, 2011. — V.2, P.ІІ. — С. 279-281.|
A new synthesis route for the production of bulk nanostructured materials is presented.
Fine Ni powder was made by selected appropriate electrolysis conditions. A
compact material with an average grain size below 40 nm was obtained by subsequent
cold pressing. Then, using the high pressure torsion (HPT) deformation technique dense
bulk nanocrystalline Ni was achieved. The detailed structural investigations of the asprepared
and HPT deformed Ni powder, including X-ray diffraction (XRD) and transmission
electron microscopy (TEM), reveal in both cases the presence of a face centered
cubic (FCC) phase without presence of any oxides. Coherently scattering domain size
measurements by XRD show a value of 24 nm for the as-deposited powder and an even
smaller value of 13.5 nm after HPT deformation. In addition, optical emission spectroscopy
was employed to determine the impurity content of the obtained nanostructured
material, showing a relatively low content of 0.9 % carbon and oxygen. The microhardness
increased after deformation from (1.5 ± 0.08) GPa for the as-deposited Ni powder
to (6.6 ± 0.2) GPa for the HPT deformed Ni powder.
When you are citing the document, use the following link http://essuir.sumdu.edu.ua/handle/123456789/20619
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